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The earliest tentative evidence for iron-making is a small number of iron fragments with the appropriate amounts of carbon admixture found in the Proto-Hittite layers at Kaman-Kalehöyük and dated to 2200–2000 BC.

Akanuma (2008) concludes that "The combination of carbon dating, archaeological context, and archaeometallurgical examination indicates that it is likely that the use of ironware made of steel had already begun in the third millennium BC in Central Anatolia".

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